The contamination of (waste)water with organic pollutants, such as pharmaceuticals and dyes, is drastically increasing. Their removal process presents several difficulties, and often activated carbon (AC) is used in a filtration step. While commercial AC is often based on fossil resources, in this study, we present a new approach toward biochar from spent coffee (SC). This new AC has considerably enhanced surface areas and porosities, making it suitable for wastewater treatment. Using MgCO