An engineered aldolase enables the biocatalytic synthesis of 2'-functionalized nucleoside analogues.

 0 Người đánh giá. Xếp hạng trung bình 0

Tác giả: William R Birmingham, Sasha R Derrington, Francesco Falcioni, William Finnigan, Martin A Hayes, Rachel S Heath, Christian Schnepel, Peter D Smith, Nicholas J Turner, Matthew Willmott

Ngôn ngữ: eng

Ký hiệu phân loại: 296.09015 Judaism

Thông tin xuất bản: England : Nature synthesis , 2025

Mô tả vật lý:

Bộ sưu tập: NCBI

ID: 172226

Nucleosides functionalized at the 2'-position play a crucial role in therapeutics, serving as both small-molecule drugs and modifications in therapeutic oligonucleotides. However, the synthesis of these molecules often presents substantial synthetic challenges. Here we present an approach to the synthesis of 2'-functionalized nucleosides based on enzymes from the purine nucleoside salvage pathway. Initially, active-site variants of deoxyribose-5-phosphate aldolase were generated for the highly stereoselective synthesis of d-ribose-5-phosphate analogues with a broad range of functional groups at the 2-position. Thereafter, these 2-modified pentose phosphates were converted into 2'-modified purine analogues by construction of one-pot multienzyme cascade reactions, leading to the synthesis of guanosine (2'-OH) and adenosine (2'-OH, 2'-Me, 2'-F) analogues. This cascade allows for the control of the 2'-functional group alongside 2-stereochemistry. Our findings demonstrate the capability of these biocatalytic cascades to efficiently generate 2'-functionalized nucleosides, starting from simple starting materials.
Tạo bộ sưu tập với mã QR

THƯ VIỆN - TRƯỜNG ĐẠI HỌC CÔNG NGHỆ TP.HCM

ĐT: (028) 36225755 | Email: tt.thuvien@hutech.edu.vn

Copyright @2024 THƯ VIỆN HUTECH