Bioinspired Synthesis of (-)-Hunterine A: Deciphering the Key Step in the Biogenetic Pathway.

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Tác giả: Péter Angyal, János Daru, Bence Balázs Mészáros, Tibor Soós, Szilárd Varga, Bálint Zsigulics

Ngôn ngữ: eng

Ký hiệu phân loại: 149.2 Realism

Thông tin xuất bản: Germany : Chemistry (Weinheim an der Bergstrasse, Germany) , 2025

Mô tả vật lý:

Bộ sưu tập: NCBI

ID: 175813

A concise, bioinspired, and enantioselective synthesis of (-)-hunterine A, an odd 6/7/6/6/5 pentacyclic natural product, is described. The key step in the synthesis of this complex structure is an interim-template directed 6-exo selective epoxide ring-opening reaction, which is interwoven with a hydrolysis step of the indolenine hemiaminal template to create the unusual 7-membered azepine bridge motif. Our work not only refines the previously proposed biogenetic pathway, but also reveals the possible stereochemical prerequisite of the unique skeletal rearrangement, which provides a vantage point for understanding how (-)-hunterine A is likely to be generated in nature.
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