Renewable Terephthalates and Aromatic Diisocyanates from Galactose.

 0 Người đánh giá. Xếp hạng trung bình 0

Tác giả: Michael D Burkart, Matthew W Halloran, Aanchal Jaisingh, Roxanne Naumann, Nathan A Romero

Ngôn ngữ: eng

Ký hiệu phân loại: 341.26 +States

Thông tin xuất bản: Germany : Angewandte Chemie (International ed. in English) , 2025

Mô tả vật lý:

Bộ sưu tập: NCBI

ID: 183308

Aromatic diisocyanates, invaluable commodity chemicals for polymer manufacturing, are produced annually on megaton scales from petroleum-derived diamines via phosgenation. Existing routes toward renewable alternatives are sparse and limited by access to functionalized aromatic starting materials, such as terephthalates. Herein, we report the development of a robust route to renewable terephthalates and aromatic diisocyanates from D-galactose via Eastwood olefination and Diels-Alder cycloaddition, followed by a mild electrochemical decarboxylative aromatization. This process was developed and applied on gram-scale to synthesize terephthalates, which were transformed into aromatic diisocyanates via Curtius rearrangement in flow. We demonstrate gram-scale preparation of 1,4-phenylene diisocyanate and 2,5-toluene diisocyanate and formulation of these monomers to prepare fully renewable thermoplastic polyurethanes. Preparation of these renewable aromatic diisocyanates proceeds without the use of high-pressure gases or costly transition-metals and represents a novel route to fully renewable aromatic diisocyanates.
Tạo bộ sưu tập với mã QR

THƯ VIỆN - TRƯỜNG ĐẠI HỌC CÔNG NGHỆ TP.HCM

ĐT: (028) 36225755 | Email: tt.thuvien@hutech.edu.vn

Copyright @2024 THƯ VIỆN HUTECH