Development and validation of a combined QuEChERS and HPLC-MS/MS method for trace analysis of ten diamide insecticides in agricultural products.

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Tác giả: Linlin Guo, Jun Li, Junfeng Lu, Rongli Pang, Tao Pang, Chengkui Qiao, Fajun Tian, Caixia Wang, Hanzhong Xie, Zhenzhen Zhou

Ngôn ngữ: eng

Ký hiệu phân loại: 338.9 Economic development and growth

Thông tin xuất bản: England : Analytical methods : advancing methods and applications , 2025

Mô tả vật lý:

Bộ sưu tập: NCBI

ID: 214267

Diamide insecticides are being widely registered worldwide, yet most of them lack established maximum residue limits (MRLs) in agricultural products. In this study, we combined a QuEChERS (quick, easy, cheap, efficient, rugged, and safe) extraction method with high-performance liquid chromatography coupled to tandem mass spectrometry (HPLC-MS/MS) analysis to simultaneously identify and quantify ten diamide insecticides in seven matrices for the first time. The method was validated in accordance with SANTE/11312/2021 guidelines, including sensitivity, linearity, trueness, and precision. Excellent linearity (
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