This book discusses multiways in the porous materials. It involves materials with a large number of holes, and it highlights the synthesis, structure, and surface properties of porous materials closely related to more applications, such as support, catalyst, energy storage, chemical reactions, and optical applications. It studies the effect of the filling materials, the thermal treatments, and the porous density in the improvement of physical properties, electrical and energy efficiency, and the generation of new materials. Some synthetic process will be discussed with the effect of some parameters on the final characteristics of the prepared porous structures.