Hydrogen-Bonding Network-Enabled Terminal Selective Heteroarylation of Allenamides in Hexafluoroisopropanol.

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Tác giả: Milan Bera, Partha Sarathi Bera, Rajshekhar Karpoormath, Yafia Kousin Mirza, Sachin Balaso Mohite, Vusisizwe Ntuli, Yugendhar Soorni

Ngôn ngữ: eng

Ký hiệu phân loại: 156.2 Comparative psychology of sensory perception, movement, emotions,

Thông tin xuất bản: United States : Organic letters , 2025

Mô tả vật lý:

Bộ sưu tập: NCBI

ID: 236920

Hexafluoroisopropanol (HFIP)-mediated terminal selective heteroarylation of allenamides has been accomplished through H-bonding network-enabled substrate activation in a robust fashion. This strategy features a cascade process involving sequential nucleophilic addition followed by electrophilic heteroaromatic substitution and is well suited for late-stage functionalization of complex bioactive molecules. The elucidation of the underlying mechanism was achieved through a comprehensive combination of several control experiments, kinetic studies, isotopic labeling experiments, and the isolation of the HFIP-allenamide intermediate adduct.
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