DEVELOPMENT AND VALIDATION OF THE MAGNETIC IMMOBILIZATION TO DETERMINE PAPP-A IN HUMAN SERUM=DEVELOPMENT AND VALIDATION OF THE MAGNETIC IMMOBILIZATION TO DETERMINE PAPP-A IN HUMAN SERUM

 0 Người đánh giá. Xếp hạng trung bình 0

Tác giả: Thi Bao Bui, Bich Ngan Nguyen, Thi Kim Lien Nguyen, Van Thao Ta

Ngôn ngữ: eng

Ký hiệu phân loại:

Thông tin xuất bản: Tạp chí Khoa học - Trường Đại học Sư phạm Hà Nội: Khoa học Tự nhiên, 2024

Mô tả vật lý: tr.105

Bộ sưu tập: Metadata

ID: 246705

 The novel magnetic method used to immobilize the primary antibody in96-well polystyrene plates was investigated to determine the pregnancy-associatedplasma protein-A (PAPP-A), one of the most important protein markers inpregnancy. The optimal conditions for the immobilization are 20 μL magneticnanoparticles (0.72 mg/mL), 2μL primary antibody (30 μg/mL), and a one-stepprocess. The reaction was implemented in 40 minutes and 30 ºC. The calibrationcurve was established and the linear range shows up to 2090 mU/L. The LOQ andLOD are 7.2 and 24.0 mU/L, respectively. The reaction is non-specific for otherpregnancy hormones such as hCG and aFP even at a high level. The Passing &Bablok regression showed the linear relationship and the agreement between newand reference methods, y = a (95% CI)x + b(95% CI), a = 1.00 (0.971 to 1.019), b= 22.07 (-73.104 to 117.244), R2 = 0.999, p<
 0.001. The Bland-Altman plot alsoshowed the high concordant. The new method can be used to determine PAPP-A inthe serum sample with mild conditions, simple and time-saving reaction, highsensitivity and selectivity, and comparable results with the commercial method.The novel magnetic method used to immobilize the primary antibody in96-well polystyrene plates was investigated to determine the pregnancy-associatedplasma protein-A (PAPP-A), one of the most important protein markers inpregnancy. The optimal conditions for the immobilization are 20 μL magneticnanoparticles (0.72 mg/mL), 2μL primary antibody (30 μg/mL), and a one-stepprocess. The reaction was implemented in 40 minutes and 30 ºC. The calibrationcurve was established and the linear range shows up to 2090 mU/L. The LOQ andLOD are 7.2 and 24.0 mU/L, respectively. The reaction is non-specific for otherpregnancy hormones such as hCG and aFP even at a high level. The Passing &Bablok regression showed the linear relationship and the agreement between newand reference methods, y = a (95% CI)x + b(95% CI), a = 1.00 (0.971 to 1.019), b= 22.07 (-73.104 to 117.244), R2 = 0.999, p<
 0.001. The Bland-Altman plot alsoshowed the high concordant. The new method can be used to determine PAPP-A inthe serum sample with mild conditions, simple and time-saving reaction, highsensitivity and selectivity, and comparable results with the commercial method.
Tạo bộ sưu tập với mã QR

THƯ VIỆN - TRƯỜNG ĐẠI HỌC CÔNG NGHỆ TP.HCM

ĐT: (028) 36225755 | Email: tt.thuvien@hutech.edu.vn

Copyright @2024 THƯ VIỆN HUTECH