The State of Tennessee, in partnership with the University of Tennessee (UT) and the Oak Ridge National Laboratory (ORNL), has created the RevV! Manufacturing voucher program to help Tennessee manufacturers gain access to the world-class resources at ORNL. As a part of this program, ORNL was working with Proton Power, Inc. (PPI), a rapidly growing company located in Lenoir City, Tennessee. PPI has developed a patented renewable energy system that uses biomass and waste sources to produce inexpensive hydrogen gas or synthetic fuels which are economically competitive with fossil fuels. The pyrolysis process used by PPI in their manufacturing chain generates significant amounts of black carbon char as by-product. The scope of ORNL collaboration with PPI was assessing the black carbon char as a potential feedstock for activated carbon production, as this could be a potentially new revenue stream. During 2015-2016 ORNL received eight char samples from PPI and characterized their initial properties, simulated their physical activation by carbon dioxide, prepared gram-size samples of physically activated carbons, and characterized their surface and porosity properties. This report presents a summary of the work methods employed and the results obtained in the collaborative project between ORNL and PPI.