Hydro-static behaviour of highly inert Fomblin and Halocarbon fluids as pressure-transmitting media in high-pressure experiments.

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Tác giả: Nico Giordano, Matic Lozinšek, Klemen Motaln, Simon Parsons, Erik Uran

Ngôn ngữ: eng

Ký hiệu phân loại:

Thông tin xuất bản: United States : Journal of applied crystallography , 2025

Mô tả vật lý:

Bộ sưu tập: NCBI

ID: 463783

A pressure-transmitting medium (PTM) plays an important role in diamond anvil cell (DAC) experiments as it ensures that the sample is exposed to hydro-static pressure. Although PTMs that are liquids under ambient conditions are the easiest to handle and load, the selection of chemically inert liquid media with established hydro-static properties is limited. To widen the choice of highly inert PTMs for high-pressure experiments, the hydro-static behaviours of Fomblin Z60, Fomblin Z25, Fomblin Y LVAC 06/6 and Halocarbon Oil 11-14 were investigated. The ruby fluorescence method was used to monitor the evolution of pressure gradients across the DAC sample chamber during compression and decompression. Fomblin Z60 and Fomblin Z25 perfluoro-polyethers, which are hydro-static to 1.7 and 1.5 GPa, respectively, exhibited the best hydro-static performance, followed by Halocarbon Oil 11-14 with a limit of 1.2 GPa, whereas the non-hydro-static behaviour of Fomblin Y LVAC 06/6 was observed above only 0.6 GPa.
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