Nghiên cứu định lượng một số hoạt chất nhóm iridoid và phenolic trong dược liệu kim ngân bằng sắc ký lỏng hiệu năng cao

 0 Người đánh giá. Xếp hạng trung bình 0

Tác giả: Văn Mến Chử, Đức Long Đào, Sĩ Thịnh Ngô, Đức Thiện Nguyễn, Duy Bắc Nguyễn, Bình Dương Vũ

Ngôn ngữ: vie

Ký hiệu phân loại: 641.657 Food and drink

Thông tin xuất bản: Y học Việt Nam, 2014

Mô tả vật lý: 56-60

Bộ sưu tập: Metadata

ID: 563553

 Lonicerae Folium et Caulis is a commonly used anti-inflammatory herbal drug. The therapeutic effectiveness of this drug depends significantly on the geographical origin, hence, the standardization using the chemical characteristics would be very important. In the present study, an HPLC method for simple and effective analysis of four main components like coniferin, acid loganic, swerosid and loganin from the Lonicerae Folium et Caulis sample was developed and validated. Four main components were base line separated on a Optimapak C18 column with gradient of mobile phase A (10 percent methanol containing 0.1 percent formic acid) and B (90 percent methanol containing 0.1 percent formic acid) for 0 min 0 percent B, 15 min 30 percent B, 25 min 70 percent B, 30 min 70 percent B, 35 min 100 percent B
  45 min 100 percent B
  50 min 0 percent B. The flow rate was 1.0 ml/min and detection was carried out at 254 nm. Methylparaben was used as an internal standard. The quantitation results showed that the highest concentrations of coniferin, acid loganic, swerosid, loganin in the analyzed samples were 0.55, 10.9, 4.22, and 7.08 mg/g and lowest concentrations were 0.03, 0.30, 0.37, and 0.02 mg/g, respectively.
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