Tổng hợp các hạt nano vật liệu tổng hợp từ tính tạo màng bao trong các đồng polyner đặc thù cho các ứng dụng ức chế theo mức

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Tác giả:

Ngôn ngữ: vie

Ký hiệu phân loại: 541.378 Magnetochemistry

Thông tin xuất bản: Advances in Natural Scienses: Nanoscience and nanotechnology, 2013

Mô tả vật lý: 45298

Bộ sưu tập: Metadata

ID: 565081

The authors report the synthesis of magnetic iron oxide nanoparticles encapsulated in maleic acid-2-acrylamido-2-methyl-I-propanesulfonate based polymer. This composite nanoparticle is specified for the high-pressure/high-temperature (HPHT) oilfield scale inhibition application. The process includes a facile-ultrasound-supported addition reaction to obtain iron oxide nanoparticles with surface coated by oleic acid. Then via inverse microemulsion polymerization with selected monomers, the specifically designed copolymers have been formatted in nanoscale. The structure and morphology of obtained materials were characterized by transmission electron microscopy (TEM), x-ray powder diffraction (XRD), Fourier transform infrared spectroscopy (FTIR) and the thermal stability. The effectiveness of synthesized compounds as a carbonate scale inhibitor was investigated by testing method NACE standard TM 03-074-95 at aging temperature of 70,90 and 120°C. The magnetic nanocomposite particles can be easily collected and detected demonstrating their superior monitoring ability, which is absent in the case of conventional copolymer-based scale inhibitor.
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