Base Mediated

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Tác giả: Mina Asadi, Mohammad Mahdavi, Rozita Yazzaf

Ngôn ngữ: eng

Ký hiệu phân loại: 594.38 *Pulmonata

Thông tin xuất bản: United Arab Emirates : Current organic synthesis , 2025

Mô tả vật lý:

Bộ sưu tập: NCBI

ID: 57756

INTRODUCTION: 1,4-oxazepine is a significant structural motif found in several bio-active molecules used in the treatment of diseases such as psychotic disorders. METHODS: Therefore, developing novel methodologies for its preparation is of great interest to medicinal chemists. RESULTS: These seven-membered heterocycles are generated through the intramolecular cy-clization of Betti bases, which are propargylated using propargyl bromide as the source of the triple bond in the presence of a base. CONCLUSION: This efficient and straightforward protocol proceeds under mild, metal-free conditions and has been shown to be applicable to a broad range of aldehydes and 2-aminopyridines.
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