Three megastigmanes. bridelionoside B (1), (3S,.5R,6R,7E, 9S )-megastigmane-7-ene-3,5,6,9-tetrol (2), and dihydroalangionoside A (3), and one phenylpropane glucoside, syringin (4) were isolated from the methanol extract of Ficus microcarpa leaves. Their structures were elucidated by spectroscopic methods including ESI-MS, ID- and 2D-NMR in comparison with the literature values.