The Ni-TiO2 composite was perfomed from nickel chloride solution by coelectrodeposition. Effect of stirring rate, current density, kind of current, electrodeposition time and concentration of TiO2 in the solution on the codeposition of the particle in the nanocomposite coating was investigated. The composition of coatings was characterized with energy dispersive analyzer system (EDX). Results showed that, the amount of nano-TiO2 embedded in coatings depended on these factors. When the amount of nanoparticles in bath of electrochemical was 6 g/l, the codeposition of the TiO2 particle in the matrix reached 10.53 percent at current density 3A/dm2, stirring rate of 600 rpm and 20 minutes electrodeposition.