Three compounds: alpha,beta-dilinoleostearin (1), 1-heptacosanol (2), 2-(4' -hydroxyphenylethyl)triacontanoate (3) along with betulinic acid and beta-sitosterol were isolated from n-hexane- and ethyl acetate- extracts of Adenosma caeruleum R.Br. Their structures were elucidated by analysis of MS, NMR spectra and comparison with the published data. This is the first report on the isolation of compounds 1,2 and 3 from Adenosma genus.