PPh3/Isocyanide and N2/Isocyanide Exchange: Pathways to Isolable Alkali Metal Keteniminyl Anions.

 0 Người đánh giá. Xếp hạng trung bình 0

Tác giả: Arpan Das, Prakash Duari, Kai-Stephan Feichtner, Gernot Frenking, Viktoria H Gessner, Sunita Mondal, Yihao Zhang, Lili Zhao

Ngôn ngữ: eng

Ký hiệu phân loại: 133.594 Types or schools of astrology originating in or associated with a

Thông tin xuất bản: Germany : Angewandte Chemie (International ed. in English) , 2025

Mô tả vật lý:

Bộ sưu tập: NCBI

ID: 693948

Keteniminyl anions hold significant promise for advancing ketenimine chemistry, yet their isolation has remained elusive until now. Drawing inspiration from recent advances in ligand exchange reactions at carbon, we report the successful synthesis of isolable alkali metal keteniminyl anions through substitution of the phosphine ligand in metalated ylides or the N2 ligand in a diazomethanides with isocyanides. The exchange reactions were found to proceed more rapidly with aryl isocyanides than with the more electron-rich alkyl-substituted derivatives and were also more efficient when starting from the diazo compounds. The resulting keteniminyl anions exhibit bent geometries, which can be attributed to a donor-acceptor interaction with the isocyanide, giving rise to a carbone-like structure. Electron-withdrawing substituents on the nitrogen enhance backbonding, thus leading to larger bending angles and a more pronounced ynamide character as also evidenced by a red-shifted of the ketenimine stretch in the IR spectrum. The keteniminyl anions react efficiently with unsaturated compounds to form a diverse array of heterocycles, highlighting their potential as versatile building blocks in synthetic chemistry.
Tạo bộ sưu tập với mã QR

THƯ VIỆN - TRƯỜNG ĐẠI HỌC CÔNG NGHỆ TP.HCM

ĐT: (028) 36225755 | Email: tt.thuvien@hutech.edu.vn

Copyright @2024 THƯ VIỆN HUTECH