Reduced graphene oxide (rGO) was synthesized by chemically reducing graphene oxide (GO) using a reducing agent. The product, rGO, showed excellent hydrophobicity, as indicated by its high-water contact angle, which was greater than 150°. Characterizations using Fourier-transform infrared (FTIR) spectroscopy, Raman spectroscopy, and X-ray diffraction (XRD) were used to analyze the composition and structural differences between GO and the superhydrophobic rGO material. Scanning electron microscopy (SEM) showed that GO particles exhibited a plate-like morphology with layers of stacked plates, while rGO displayed fewer stacks that show a more separated structure of layers. The increasing demand for superhydrophobic materials in advanced materials industries, due to their potential to enhance performance, durability, and safety, makes rGO a promising candidate for use in composite materials.