Unlocking Reactivity of Unprotected Oximes via Green-Light-Driven Dual Copper/Organophotoredox Catalysis.

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Tác giả: Xiaoming Jie, Jiawen Lai, Yaping Shang, Weiping Su, Mengqi Wang, Shuping Wang

Ngôn ngữ: eng

Ký hiệu phân loại: 785.13 *Trios

Thông tin xuất bản: Germany : Angewandte Chemie (International ed. in English) , 2025

Mô tả vật lý:

Bộ sưu tập: NCBI

ID: 718198

Oximes are widely used precursors in synthetic chemistry due to their broad availability and versatile chemical properties, in which N─O bond fragmentation represents a key reactivity mode. However, these transformations typically require the use of oxygen-protected oximes, and a general strategy to directly utilize free oximes remains challenging due to their vulnerability to side reaction pathways, rendering low tendency towards N─OH bond cleavage. Here a unified platform is reported to achieve direct cyclization of unprotected oximes with enals, as well as other coupling partners through dual copper/organophotoredox catalysis under green light irradiation. This protocol enables concurrent activation of both N─OH and α-C(sp
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