Concise first total synthesis of phenylethanoid glycosides parvifloroside A and crassifolioside.

 0 Người đánh giá. Xếp hạng trung bình 0

Tác giả: Zaher M A Judeh, Duc Thinh Khong, Madhu Babu Tatina

Ngôn ngữ: eng

Ký hiệu phân loại:

Thông tin xuất bản: Netherlands : Carbohydrate research , 2025

Mô tả vật lý:

Bộ sưu tập: NCBI

ID: 718256

The first total synthesis of phenylethanoid glycosides parvifloroside A 1 and crassifolioside 2 is disclosed, achieving excellent 31 % and 33 % overall yield, respectively. The synthesis exploited the inherent reactivity differences among the free hydroxyl groups on 4-O-caffeoyl glucopyranoside 3 intermediate, enabling regioselective caffeoylation and rhamnosylation. The key to the synthesis is using chiral 4-pyrrolidinopyridine organocatalyst 6 to achieve the regioselective caffeoylation and migration of acyl groups. Notably, the synthesis avoids the common challenge of E:Z isomerization of the caffeoyl moiety's double bond. Additionally, only a single protection/deprotection step is employed, significantly simplifying the process. This concise approach provides a practical route to these natural products and establishes a versatile strategy for synthesizing a wide array of phenylethanoid glycosides with similar substitution patterns.
Tạo bộ sưu tập với mã QR

THƯ VIỆN - TRƯỜNG ĐẠI HỌC CÔNG NGHỆ TP.HCM

ĐT: (028) 36225755 | Email: tt.thuvien@hutech.edu.vn

Copyright @2024 THƯ VIỆN HUTECH