Design and Synthesis of Pyridopyrimidines Targeting NEK6 Kinase.

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Tác giả: Marianna Buttarelli, Natalia Cappoli, Marta De Donato, Maria Cristina De Rosa, Ðorđević Luka, Juan José Galano-Frutos, Daniela Gallo, Matteo Gramanzini, Anna Königs, Michele Maggini, Davide Pirolli, Benedetta Righino, Viviana Romano, Giovanni Scambia, Alessandro Semeraro, Paolo Zardi

Ngôn ngữ: eng

Ký hiệu phân loại:

Thông tin xuất bản: United States : Archives of biochemistry and biophysics , 2025

Mô tả vật lý:

Bộ sưu tập: NCBI

ID: 718698

We designed a series of pyrido[2,3-d]pyrimidine derivatives based on the structure of the NEK6 kinase inhibitor, compound 21 (2-amino-5-phenyl-5,11-dihydro-3H-indeno[2',1':5,6]pyrido[2,3-d]pyrimidine-4,6-dione), which share the same heterocyclic core. Chemical modifications, aimed at altering the molecular planarity of 21 to enhance water solubility, were guided by receptor-based ligand design and further supported by molecular docking, molecular dynamics simulations, and free energy perturbation calculations. Our results indicate that disrupting the planarity of 21 increases aqueous solubility - nearly doubling it in two cases- while reducing lipophilicity. Among the compounds tested, three showed both improved solubility and NEK6 inhibitory activity exceeding 50% in single-dose assay.
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