Radical Chemistry of Tetrazenes: Access to Polymers with Pristine Tetrazenyl Chain Ends and Depolymerization Applications.

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Tác giả: Anne Baudouin, Laetitia Bourgeois, Lucas Chalouni, Emmanuel Chefdeville, Chaza Darwich, Ahmad Hammoud, Lhoussain Khrouz, Emmanuel Lacôte, Jennifer Lesage de la Haye, Jean Raynaud, Anne Renault

Ngôn ngữ: eng

Ký hiệu phân loại: 541.382 Radiation chemistry

Thông tin xuất bản: Germany : Angewandte Chemie (International ed. in English) , 2025

Mô tả vật lý:

Bộ sưu tập: NCBI

ID: 742316

We report the first radical reaction of tetrazenes- i.e., functions with four consecutive nitrogen atoms with a linear N-N═N-N chain-that retains the characteristic 4N pattern. Selective hydrogen atom transfer (HAT) in the α-position of the 4N chain enables the free radical polymerization of various polar and nonpolar monomers. The tetrazene units play a dual role. Its decomposition generates aminyl radicals that can undergo HAT with another tetrazene molecule and lead to initiating C-centered radicals. Contrary to what was previously thought the aminyl radicals never add to the monomers. The polymers obtained feature tetrazene chain ends, which can be harnessed as macro-initiators to further grow the polymer chains. Heating of the former above the ceiling temperature leads to cleavage of the tetrazene function, which enables depolymerization by unzipping of polymethyl methacrylate (PMMA) and polystyrene (PS).
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