Mechanical Rejuvenation of Polylactide: Critical Role of Mobile Amorphous Phase.

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Tác giả: Peng Chen, Wei Huang, Xuke Li, Shenying Sun, Jian Zhou

Ngôn ngữ: eng

Ký hiệu phân loại: 133.594 Types or schools of astrology originating in or associated with a

Thông tin xuất bản: Germany : Macromolecular rapid communications , 2025

Mô tả vật lý:

Bộ sưu tập: NCBI

ID: 753595

Polylactide (PLA) becomes brittle shortly after physical aging, posing significant challenges for practical applications. This issue can be effectively overcome through a pre-melt-stretching process, known as mechanical rejuvenation. However, the underlying mechanisms remain poorly understood due to the intricate multilevel structures in pre-stretched PLA and their evolution during physical aging. Herein, PLA containing 12% D-isomer units is utilized as a model system to eliminate the influence of structures such as mesophase and crystals. The samples remain fully amorphous throughout the pre-stretching and subsequent aging processes. Notably, during physical aging, the pre-stretched samples retain their ductility, while the isotropic samples exhibit increased embrittlement. Thermal analysis is employed to elucidate the changes in the amorphous phase during aging. The results reveal the impact of the amorphous segmental mobility on the ductility change during aging, which is primarily governed by the fraction of mobile amorphous phase (X
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